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1 edition of separation and characterization of nitrogen heterocyclic compounds present in coke-oven pitch. found in the catalog.

separation and characterization of nitrogen heterocyclic compounds present in coke-oven pitch.

separation and characterization of nitrogen heterocyclic compounds present in coke-oven pitch.

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Published by British Carbonization Research Association in Chesterfield .
Written in English


Edition Notes

SeriesCarbonization research report -- 101
ContributionsBritish Carbonization Research Association.
ID Numbers
Open LibraryOL14308576M

Separation and identification of heterocyclic nitrogen compounds in biooil derived by fast pyrolysis of chicken manure. Kazi ZH(1), Schnitzer MI, Monreal CM, Mayer P. Author information: (1)Eastern Cereal and Oilseed Research Center, Agriculture and Agri-Food Canada, Ottawa, Canada.   It’s necessary to extract nitrogen from the air so that it can be used in a purified state. 2 Methods for Achieving Nitrogen Separation from Air. To do this, air-separation plants and nitrogen generators are used. There are three methods for the separation of air components: PSA, membrane, and cryogenic systems.

  The high-pressure separation of carbon dioxide/nitrogen and carbon dioxide/hydrogen mixtures was investigated over two phenolic-resin-derived activated carbon bead samples: an unmodified activated carbon made from a phenolic resin precursor and a modified material manufactured by treating the former activated carbon with first nitric acid and then ammonia. The alkylphenol compounds present in a coal-derived liquid have been separated by this method. to allow for a comprehensive characterization of nitrogen compounds in diesel and related samples.

Nitrogen heterocycles represent a highly important class of compounds that are widespread in medicinal chemistry, receiving special attention in drug discovery. These heterocyclic rings are common structural units in many natural or synthetic agents and approximately 60% of FDA-approved drugs contain a nitrogen heterocycle in their structure. In the separation of feed oils by aqueous methanol solution as solvent, nitrogen heterocyclic compounds in the absorption oil and the tar light oil were extracted preferentially to other compounds.


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Separation and characterization of nitrogen heterocyclic compounds present in coke-oven pitch Download PDF EPUB FB2

Journal of Chromatography, () Elsevier Science Publishers B.V., Amsterdam - Printed in The Netherlands CHROM. 19 SEPARATION AND CHARACTERIZATION OF NITROGEN HETEROCYCLE AND HYDROXYL AROMATIC COMPOUNDS IN NON-DISTILLABLE COAL-DERIVED LIQUIDS STEPHEN C.

RUCKMICK and ROBERT J. HURTUBISE* Department of Chemistry Cited by: 6. (). Separation of heterocyclic nitrogen compounds from coal tar fractions via ionic liquids: COSMO-SAC screening and experimental study.

Chemical Engineering Communications: Vol.No. 9, pp. Cited by: 4. In addition to PAH, heterocyclic compounds containing oxygen, nitrogen and sulfur are also present in small amounts. Although the reaction of a representative model compound provides useful information on the mechanism of coal tar pyrolysis, it is.

Heterocyclic nitrogen compounds. Part I. Derivatives of 7: diazanaphthacene. Hatt and (Miss)E. Stephenson Abstract. The first page of this article is displayed as the abstract. Fig. 1 illustrates the separation scheme of the basic nitrogen compounds from the VGO and VGO-HT. First, about 10 g of the VGO sample or 25 g of the VGO-HT sample were dissolved in 50 mL or mL of n-hexane, respectively.

Then, g or g of FeCl 3 were added to the solutions, respectively. The mixtures were stirred vigorously at 80 °C for 3 h, and the coordination complexes Cited by: 2.

References p OTHER NON-HETEROCYCLIC NITROGEN COMPOUNDS A cation-exchange resin with a low degree of cross-linking (Dowex 50W-X2) was used for the separation in order to improve the accessibility of the ion-exchange phase to the large molecules of the derivatives and to accelerate the diffusion rate in the resin.

The separation of four kinds of nitrogen heterocyclic compounds (NHCs) from a model mixture comprising NHCs (indole (In), quinoline (Q), iso-quinoline (iQ), quinaldine (Qu)), three kinds of.

past decades, compounds bearing heterocyclic nuclei have received much attention due to their chemotherapeutic value in the development of novel antimicrobials Most of the heterocyclic compounds with oxygen, nitrogen and sulfur as heteroatoms from the classes like benzimidazole, benzothiazole, benzoxazole, quinoline have displayed wide range of.

Overview: InNitrogen Heterocyclic Compounds were the world's 36th most traded product, with a total trade of $B. Between and the exports of Nitrogen Heterocyclic Compounds grew by %, from $B to $B.

Trade in Nitrogen Heterocyclic Compounds represent % of total world trade. To compare between 1 and 3, let's take into account the interaction between the non-bonding electron pair on nitrogen and the anti-bonding MO of the C-H bond (σ*C-H). In order for the interaction to be effective, the lone pair on nitrogen and the C-H bond must be planar.

In the six-membered ring, there is always a C-H bond next to the nitrogen lays in the parallel position against nitrogen's.

the environment as complex mixtures. Heterocyclic PACs, containing an oxygen, nitrogen, or sulfur atom within a ring, comprise one of the least studied groups of PACs There are few authentic standards available, and the high number of potential isomers present challenges in the separation, identification, and quantitation of these more.

The nitrogen heterocyclic and homocyclic compounds with shorter side chain and more aromatic rings contained in atmospheric residue could be removed and, thus, the total content of nitrogen compounds could be lowered by non-polar solvent extraction.

The polar solvent could extract the nitrogen compounds selectively from the liquid. Series: Advances in Nitrogen Heterocycles Heterocyclic molecules account for over half of all known organic compounds. A large proportion of these heterocyclic compounds contain nitrogen; indeed many classes of impotant natural products, as well as a majority of synthetic drugs, dyes, etc.

are based on nitrogen heterocycles. Major compounds are polycyclic aromatic hydrocarbons (PAH), and heterocyclic compounds containing oxygen, nitrogen, and sulfur are present as minor constituents.

Even though one-dimensional gas chromatography (1D-GC) is a well-established analytical technique for the analysis of coal tar, it presents drawbacks because the matrix is extremely. The emission of sulfur and nitrogen oxides to the atmosphere caused by the presence of heterocyclic sulfur and nitrogen compounds present in fuel oils, is one of the main environmental issues.

To identify the nitrogen compounds, it was necessary to locate the m.s. scan corresponding to each peak in the 0 10 20 30 40 50 60 70 Retention time (min) Figure 2 G.c.-AFD and g.c.-FID chromatograms of coke oven pitch, and boiling point calibration graph. Peak numbers refer to compounds listed in Table 4 and letters to compounds listed in Table 2.

Heterocyclic compounds of nitrogen. Part III. The synthesis of some 2′-indolylbenzoquinones Authors contributing to RSC publications (journal articles, books or book chapters) do not need to formally request permission to reproduce material contained in this article provided that the correct acknowledgement is given with the.

of halide ion on the SERS spectra of nitrogen heterocyclic compounds at various pH values. Journal of Electroanalytical Chemistry and Interfacial Electrochemistry.

[10] Christopher JF, Mark AW, Donald R. Monobromoborane adducts and boronium salts of some nitrogen heterocyclic compounds. Journal of Inorganic and Nuclear. Heterocyclic compounds are present in abundance in our surroundings. They owe their importance in the biological system due to uniqueness in their structural Skelton parts.

They are naturally found in nucleic acid, vitamins, antibiotics, hormones etc. Nitrogen containing heterocyclic compounds are an important class of heterocyclic compounds. A multistep synthesis of thieno[2,3-b]pyridine derivatives is described that is suitable for the upper-level undergraduate organic laboratory.

This experiment exposes students to various hands-on experimental techniques as well as methods of product characterization such as IR and 1H NMR spectroscopy, and mass-spectrometry. It also provides an opportunity for students to review important. Coal tar pitch is contacted with a promoter liquid having a 5 volume percent distillation temperature of at least ° F.

and a 95 volume percent distillation temperature of at least ° F. and no greater than about ° F., with the liquid having a characterization factor of at least to promote the separation of quinoline insolubles from the pitch.This review article has a list of Nitrogen containing heterocyclic compound or drugs which are employed in the treatment of different Cardiovascular disease.

It includes name of the drugs along with their mechanism of action & structures. S. No Name of Drug Structure Mechanism of action 1 Nifedipin.Nevertheless, Li et al. [9, 10] argued that the effect of structure and composition of basic nitrogen compounds was much more obvious than that of nitrogen content.

Consequently, the characterizing nitrogen compounds in CGO and investigating the nitrogen compounds how to deactivate FCC catalysts have become research hotspots.